Chromatography

The LCPO has a strong expertise in chromatographic technics dedicated to polymers :
- Separation and structural identification (HPLC, GC-MS, LC-MS)
- Absolute and relative molar mass determination and polydispersity (SEC RI-UV-MALS)
- Polymers purification (Flash chromatography)
- Follow-up and development of organic syntheses (HPLC)

EquipmeNTS:

  • Flash chromatography Reverlis PREP (BUCHI) –  Evaporative Light Scattering Detector and UV detector
  • High Performance Liquid Chromatography - Corona and UV detectors (Thermoscientific)
  • Liquid chromatography - Mass Spectrometer detector (Thermoscientific)
  • Gas-chromatography - Mass Spectrometer detector (Thermoscientific)
  • Gas-chromatography - Flame Ionisation Detector (Thermoscientific)
  • Size Exclusion Chromatography (Thermoscientific) with Multi Angle Light Scattering (Wyatt Technology), Differencial Refractive Index (Wyatt Technology) and Diode Array Detectors (Thermoscientific) :
    - One device in THF
    - One device in DMF or DMSO
    - One device in Toluene or HFIP
    - One device in aqueous buffer
  • Size Exclusion Chromatography (Malvern Panalytical) with Refractometer, Viscometer, Light Scattering (2 angles) and Diode Array Detectors in CHCl3 or THF
  • High Temperature Size Exclusion Chromatography (Agilent Technologies) with Differencial Refractive Index and Viscometer detectors in TCB or DMF

Contact:

FREDERIQUE HAM-PICHAVANT

Chromatogram obtained by size exclusion chromatography